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Journal of Electron Microscopy 46(1): 23-31 (1997)
© 1997 Oxford University Press

Structure determination of YBCO fluorinated phases by HREM

G. Van Tendeloo1,*, O. I. Lebedev1, R. V. Shpanchenko2 and E. V. Antipov2

1EMAT, University of Antwerp (RUCA), Groenenborgerlaan 171 B-2020 Antwerpen, Belgium
2Department of Chemistry, Moscow State University 119899 Moscow, Russia

*To whom correspondence should be addressed

The structure of fluorinated YBa2Cu3O6Fx phases has been determined using a combination of X-ray diffraction, electron diffraction, high-resolution electron microscopy and microanalysis. It was unambiguously demonstrated that fluorine indeed enters the structure at the oxygen positions of the Cu(1) plane. The structure of the fully fluorinated phase YBa2Cu3O6F2 is mainly deduced from high-resolution electron microscopy.

Keywords     high-resolution electron microscopy,, YBCO fluorinated phases

Received     24 September 1996, accepted 15 October 1996


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