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Journal of Electron Microscopy 46(1): 45-47 (1997)
© 1997 Oxford University Press
FIB/HVEM observation of the configuration of cracks and the defect structure near the cracks in Si
Department of Quantum Engineering, Nagoya University Nagoya 464-01, Japan
Cracks were introduced in a Si bulk single crystal by a Vickers indentation and foil specimens which contain the cracks in the plane of foil were prepared using a focused ion beam technique. The configuration of the cracks and the defect structures near the indentation were observed by transmission electron microscopy at 1000 kV. The cracks were classified into two groups, a halfpenny crack and a lateral crack. The emission of dislocations near the crack tips was observed by both an in-situ heating and a post-mortem heating experiment.
Keywords focused ion beam/high-voltage electron microscopy,, silicon cracks.
Received 22 October 1996, accepted 30 October 1996