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Journal of Electron Microscopy 46(1): 79-83 (1997)
© 1997 Oxford University Press
Development of coincidence transmission electron microscope (II) Observation of coincidence electron microscopic image
Department of Applied Physics, Faculty of Engineering, Osaka University Yamadaoka 2-1, Suita, Osaka 565, Japan
A coincidence electron microscopic image was successfully observed by using signal electrons that generated characteristic X-rays (Ag L X-rays) during penetration through a specimen (a silver film). The coincidence measurement between the transmitted electrons and characteristic X-rays enables only the signal electrons to be extracted from a tremendous number of background electrons. The system for the coincidence electron microscope is composed of three parts: (1) an energy dispersive type Si (Li) semiconductor detector for characteristic X-rays, (2) a two-dimensional position sensitive detector for transmitted electrons and (3) high speed coincidence electronic circuits. This system enabled the coincidence electron microscopic image of Ag-film to be observed with considerable success, although the spatial resolution wasrather poor. This is mainly due to the chromatic aberration of a weak lens caused by wide-energy spread of the signal electrons.
Keywords coincidence electron microscope,, elemental mapping,, low radiation damage,, characteristic X-ray,, background elimination
Received 6 August 1996, accepted 28 October 1996