Journal of Electron Microscopy 47(5): 395-405 (1998)
© 1998 Oxford University Press
Towards 0.1 nm resolution with the first spherically corrected transmission electron microscope
1CEOS GmbH Im Neuenheimer Feld 519, D-69120 Heidelberg, Germany
2Institut für Angewandte Physik, Technische Universität Darmstadt Hochschulstraße 6, D-64289 Darmstadt, Germany
3Institut für Festkörperforschung Forschungszentrum Jülich, D-52425 Jülich, Germany
*To whom correspondence should be addressed. E-mail: rose{at}ltoi.iap.physik.tu-darmstadt.de
A hexapole corrector which compensates for the spherical aberration of the objective lens has been incorporated in a commercial 200 kV transmission electron microscope (TEM) equipped with a field emission gun. The successful correction of the spherical aberration is demonstrated by decreasing the instrumental resolution limit from 0.24 nm down to about 0.13 nm. Images of Si-SiCO2 interfaces obtained with the corrected TEM show a remarkable suppression of artefacts and a strong increase in contrast apart from the improved resolution. The design, alignment and the performance of the corrected instrument are outlined in detail.
Keywords aberration correction, reduction of artefacts, information limit, contrast enhancement, point spread function, high-resolution TEM
Received 2 April 1998, accepted 26 June 1998
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