Journal of Electron Microscopy Advance Access originally published online on January 5, 2008
Journal of Electron Microscopy 2008 57(1):13-18; doi:10.1093/jmicro/dfm037
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Electron holography study for two-dimensional dopant profile measurement with specimens prepared by backside ion milling
1 New Technology & Analysis Division, National Nanofab Center, Daejeon 305-806, Korea
2 Department of Materials Science & Engineering, Korea Advanced Institute of Science and Technology, Daejeon 305-701, Korea
3 Semiconductor Device Lab, Samsung Advanced Institute of Technology, Yongin 446-712, Korea
4 Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, Katahira 2-1-1, Sendai 980-8577, Japan
* To whom correspondence should be addressed. Tel: +82-42-879-9555; Fax: +82-42-879-9609; E-mail: jhyoo{at}nnfc.com
The visualization of two-dimensional dopant profiles and the quantitative analysis of the built-in potential across the p–n junction,
Vp-n, by electron holography were carried out with specimens prepared from the backside ion milling method combined with the focused ion beam technique. It was possible to obtain dopant profiling of the large field of view with low surface damage and gradually changed thickness. From the quantitative analysis using the phase information of electron holography and the thickness information of electron energy-loss spectroscopy,
Vp-n was estimated to be about 0.78 V assuming that the thickness of the dead layer on both surfaces is 50 nm, which is to show the difference of within 12% from the calculated value. It demonstrates that the backside ion milling method is a very promising specimen preparation technique for the reliable and quantitative analysis of dopant profiling with electron holography.
Keywords electron holography, quantitative analysis of 2D dopant profile, backside ion milling, p–n junction, electron energy-loss spectroscopy, focused ion beam
Received 16 September 2007, accepted 4 December 2007
** Shaislamov Ulugbek is doctoral course student of Kumoh National Institute of Technology, Gumi, 730-701, Korea.