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Journal of Electron Microscopy 2008 57(2):53-57; doi:10.1093/jmicro/dfn003
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© The Author 2008. Published by Oxford University Press on behalf of Japanese Society of Microscopy. All rights reserved. For permissions, please e-mail: journals.permissions@oxfordjournals.org

Characterization of the charging effect in a ZrO2 sintered body by Ga ion beam irradiation

Ki Hyun Kim1, Joong Jung Kim1,3,, Toshiaki Suzuki2 and Daisuke Shindo1,*

1 Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, Sendai 980-8577 and
2 JEOL Ltd., 3-1-2 Musashino, Akishima, Tokyo 196-8558, Japan
3 Present address: Initial Research Project, Okinawa Institute of Science and Technology, c/o Hitachi Advanced Research Laboratory, Akanuma 2520, Hatoyama, Saitama 350-0395, Japan

* To whom correspondence should be addressed. E-mail: shindo{at}tagen.tohoku.ac.jp

The charging effect in a ZrO2 sintered body was investigated by using scanning ion microscope (SIM) images. In this study, we report interesting features caused by the charging effect in the ZrO2 sintered body during the Ga ion beam irradiation: a bright contrast with a distorted net shape appears around the positively charged specimen. From this feature in the SIM image, it is clarified that the Ga ion beam is strongly deflected and the wide area of the internal parts of the focused ion beam machine is irradiated by the Ga ion beam, depending on the extent to which the specimen is charged. We discuss the mechanism of the characteristic charging effect through observing SIM images by varying the intensity of the Ga ion beam.

Keywords     charging effect, secondary electron, Ga ion beam irradiation, focused ion beam

Received     16 November 2007, accepted 31 January 2008


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