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Journal of Electron Microscopy 48(4): 367-373 (1999)
© 1999 Oxford University Press

High-resolution transmission electron microscopy of Fe-Al powder particles

Makoto Shiojiri1,*, Masahiro Kawasaki2, Mari Fujii3, Katsuhiko Wakayama3 and Tadanori Yoshioka4

1Kyoto Institute of Technology Kyoto 606-8585, Japan
2JEOL Co. Ltd Akishima 196-8558, Japan
3Materials Research Center TDK Co. Ltd, Narita 286-8588, Japan
4JEOL High-Tech Inc. Akishima 196-8558, Japan

*To whom correspondence should be addressed. E-mail: shiojiri{at}pc4.so-net.ne.jp

Sections of a few µm-sized particles of Fe1–xAlx (x = 0.35–0.42) powders, produced by the atomizing method, were prepared for transmission electron microscopy (TEM) using new specimen supporting methods and ion thinning. As-atomized paramagnetic particles, the particles magnetized by cold milling for several hours and those demagnetized by ageing for 1 min at 200°C have been observed in cross-sectional high-resolution TEM images.

Keywords     TEM specimen preparation, HRTEM, fine particle, Fe-Al alloy

Received     16 October 1998, accepted 27 April 1999


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